芍丹乙肝颗粒澄清工艺的研究
芍丹乙肝颗粒,,芍丹乙肝颗粒；澄清工艺；ZTC1+1天然澄清剂,1仪器与试药,2方法与结果,3结论,参考文献：
摘要：目的：优选芍丹乙肝颗粒的澄清工艺。方法：分别采用高速离心法、乙醇沉淀法、吸附澄清技术对芍丹乙肝颗粒进行除杂，以水浸出物收率、总多糖保留率及芍药苷保留率作为评价指标，并与自然沉降法进行比较。结果：3种澄清工艺对3个指标均有不同程度的影响，其中吸附澄清技术中加入4%药液量B组分和8%药液量A组分的正天成(ZTC)1+1Ⅱ型天然澄清剂，能使水浸出物收率降至18%左右，有效成分保留率分别在80%和90%以上。结论：吸附澄清技术中加入ZTC1+1Ⅱ型天然澄清剂可作为芍丹乙肝颗粒的澄清工艺。关键词：芍丹乙肝颗粒；澄清工艺；ZTC1+1天然澄清剂
Study on clarification process of Shaodanyigan Granule
ZHAO Jun，LI Dongfeng，ZHANG Fan，et al
(Department of Pharmacy，First Affiliated Hospital，Xinjiang Medical University，Urumuqi 830054，China)
Abstract：Objective：To choose the best clarification process of Shaodanyigan Granule.Methods：By determinating dry extract percent，total polysaccharide content and paeonoside content，three clarification processes including highspeed centrifugal，ethanal precipitation，adsorption clarification technique were compared with nature sedimentation.Results：Three clarification processes had different level effect on the three index.Among them adsorption clarification technique could reduce the dry extract percent to around 18% and make the retention rate of the active components above 80% and above 90% ......
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