氢地油乳剂的制备与含量测定
醋酸泼尼松,,醋酸泼尼松；地卡因；氢地油乳剂；含量测定,1仪器和试剂,2方法与结果,3讨论,参考文献:
摘要：目的：用双波长分光光度法测定氢地油乳剂中醋酸泼尼松和盐酸地卡因含量。方法：分别选择238 nm为醋酸泼尼松的测定波长，327 nm为参比波长,在308 nm处直接测定盐酸地卡因的吸收度。结果：醋酸泼尼松和盐酸地卡因在5 ～ 15 μg / ml范围内吸收度与浓度均呈良好的线性关系(r=0.999 3，r=0.999 9)，两种组分的平均回收率和RSD值分别为98.42%、0.95% 和99.81%、0.56%。结论：用双波长分光光度法测定氢地油乳剂中的醋酸泼尼松和盐酸地卡因含量，方法简便准确，样品无需分离即可直接测定，乳剂中的其它组分对测定没有干扰。关键词：醋酸泼尼松；地卡因；氢地油乳剂；含量测定
Preparation and determination of Qindiyou emulsion
Abdukeyim, ZHANG Maohui, Dilidaer
(College of Pharmacy，First Affliated Hospital，Xinjiang Medical University,Urumqi 830054, China)
Abstract: Objective：To establish the assay method and quality specification of Qindiyou emulsion. Method：The concentration of Dicaine in Qindiyou emulsion was determined directly with dualwavelength spectrophotometry，the determination wavelength was 308 nm, in the meanwhile ......
您现在查看是摘要页，全文长 7075 字符。