新黄皮酰胺酮_____新黄皮酰胺酮；热稳定性；热分解机理

外消旋新黄皮酰胺酮的热稳定性研究

http://www.100md.com 《广东药学院学报》 2005年第2期

新黄皮酰胺酮,,新黄皮酰胺酮；热稳定性；热分解机理,1实验部分,2结果,3讨论,参考文献

     摘要用差示扫描量热法(DSC)和热重分析(TG)两种热分析方法研究外消旋新黄皮酰胺酮的热稳定性及热分解过程。在氮气氛(氮气流量为20 mL/min)、10 K·min-1的升温条件下，外消旋新黄皮酰胺酮固体在232~335 ℃之间发生激烈的分解反应，至475 ℃时分解完全。

    关键词新黄皮酰胺酮；热稳定性；热分解机理

    Thermostability of racemic neoclausenamidone

    LIN Hansen1, ZHANG Yanmei1,XU Ruimei2

    (1. Department of Medicinal Chemistry, Guangdong College of Pharmacy, Guangzhou 510240, China； 2. Instrumentation Analysis and Research Center, Sun Yatsen University, Guangzhou 510060, China)

    Abstract The thermal decomposition of racemic neoclausenamidone was studied using differential scanning calorimetry and thermogravimetry. Neoclausenamidone decomposed rapidly between 232 ℃ and 335 ℃ in the nitrogen stream with a heating rate of 10 K·min-1. Complete decomposition happened at the temperature up to 475 ℃ ......

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