HPLC法测定心舒宝片中丹酚酸B的含量
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【中图分类号】R917
【文献标识码】A
【文章编号】1672-5085(2007)07-0104-02
【摘要】目的:建立高效液相色谱法测定心舒宝中丹酚酸B的含量。方法:选用Hypersil-ODS(5um,250mm×4mm),甲醇-乙腈-1%甲酸(27∶10∶63)为流动相,柱温30℃,检测波长286nm。结果:线性范围为0.1725~8.6250ug(r=0.9995)。平均回收率99.12%,RSD=1.26%。结论:本方法简便易行,分离效果好,可用于本品质量控制。
【关键词】高效液相色谱法 心舒宝 丹酚酸B
HPLC method measurement XinShuBaopiece the content ofDan phenolic acid B.Wu Qingzhen
【Abstract】Purpose:Establishment efficiently liquid mutually color table method measurement the content of Dan phenolic acid B in the XinShuBao.Method:Choose Hypersil-ODS(5 um, the 250 mm × 4 mm), the methanol-methy1 cyanide- 1%formic acid(27 ∶ 10 ∶ 63)be flow mutually, pillar be 30 ℃ , examination wave-length 286 nm.Result:Line scope's 0 1725~8 . 6250 ugs.(r=0 . 9995)Average recovery rate 99 12%, RSD=1 26%.Conclusion:This method is simple easy line, separate effective, can used for this quality quantity control.
【Key words】Efficiently liquid mutually the color table methodXinShuBao Dan phenolic acid B
心舒宝片是由丹参、白芍 、刺五加、郁金、山楂等中药精制而成的中药制剂 ......
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