摘 要：本文采用气相色谱-三重四极杆串联质谱结合多反应监测模式，建立了一种快速测定植物油中17种邻苯二甲酸酯的检测方法。试验采用含饱和正己烷的乙腈超声提取、低温冷冻离心方式对前处理条件进行优化。结果表明，17种邻苯二甲酸酯在20～1 000 μg·L-1线性关系良好，相关系数均大于0.995，方法检出限为1.37～36.8 μg·kg-1。加标回收率为85.9%～108.4%，精密度为0.79%～8.30%。该方法前处理简单快速，回收率和精密度较高，可用于植物油中17种邻苯二甲酸酯含量的快速测定。

    关键词：气相色谱-串联质谱法；邻苯二甲酸酯；快速检测

    Abstract： This article uses gas chromatography triple quadrupole tandem mass spectrometry with multi reaction monitoring mode to establish a rapid detection method for 17 phthalates in vegetable oil. The experiment used acetonitrile with saturated n-hexane for ultrasonic extraction and low-temperature freeze centrifugation to optimize the pretreatment conditions. The results showed that there was a good linear relationship between 17 phthalates in the range of 20～1 000 μg·L-1 ......